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Electrokinetic and in situ UV-Vis spectroscopic analyses suggest that redox energetic nickel hydroxide types is made at first glance of NiO electrocatalysts during HMF oxidation, and also this Ni(II) hydroxide oxidation to Ni(III) oxyhydroxide step could be the price deciding step (RDS). This mechanistic research for biomass oxidation in CO2-saturated electrolyte provides insight into constructing a very efficient system for the paired electrolysis of CO2 decrease and biomass oxidation.The three-comp
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