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Au nanoparticles (AuNPs) (10-15 nm in size) were prepared and deposited on the surfaces of silica particles functionalized using 3-aminopropyltriethoxysilane as the seeds under mild conditions. Then, Au seeds grew further and formed nanosheets by the method of gold chloride hydrate reduction. 3, 5-dimethylphenyl isocyanate derivative of cellulose as chiral selector was coated on the surfaces of SiO2/Au. The obtained spheres possessed a sandwich structure in which silica bead, the packed Au NPs monolayer and cellulose derivative were the c