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To study the intraday and interday patterns and possible sources of volatile organic compounds (VOCs), 6-h active sampling was performed in April, May, June, July, and August 2017 and in January 2018 in a semi-urban site in Bolu, Turkey. Totally 69 VOCs having biogenic (BVOCs, i.e., isoprene, monoterpenes and oxygenated VOCs) and anthropogenic origins (AVOCs) were examined. Fifty-four of sixty-nine analyzed VOCs could be detected. Decanal followed by benzaldehyde, benzene, phenol, and toluene were detected as the leading anthropogenic V