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Putting such species in the context of the previously investigated hydroboration catalysis, its stoichiometric reaction with pinacolborane revealed its potential conversion into a cobalt(ii) hydride complex, thus confirming its original attribution as off-cycle species.Herein, we constructed amorphous ReS2 nanosheets anchored on TiO2 nanowires by delicately forming Ti-O-Re bonds, which exhibited considerable average ammonia yield and faradaic efficiency as high as 5.3 μg h-1 cm-2cat. and 49.8% at an applied potential of -0.2 V (vs. RHE)
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