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In the present work, the characterization and gas sensing properties of newly synthesized N-(4-methylpyrimidine-2-yl)methacrylamide (N-MPMA) monomer Langmuir-Blodgett (L thin films were investigated. The UV-visible spectroscopy, quartz crystal microbalance (QCM), and atomic force microscopy were utilized to characterize N-MPMA LB thin films. The surface behavior of N-MPMA monolayer was stable and allowed an effective transfer at a surface pressure of 14 mN/m. The mass change/unit area value of the N-MPMA LB thin film deposited quart