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X-ray photoelectron spectroscopy (XPS) results confirmed the existence of Ti3+, resulting in the formation of semiconducting parts in the bulk ceramics. Low tanδ and excellent temperature stability were due to the high resistance of the insulating layers with a very high potential barrier of ∼2.0 eV.A mixed water-organic solvent used for amidoximation increased the production cost of an amidoxime-based polymer sorbent and was not environmentally friendly as well. In this work, the amidoximation of an ultrahigh molecular weight polyethy