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In this research, the removal of sinapine had been investigated using three techniques (i) from a mustard seed meal defatted by a supercritical CO2 (SC-CO2) pretreatment, (ii) because of the utilization of high-voltage electrical discharges (HVEDs), (iii) and also by the employment of ultrasound. The employment of SC-CO2 pretreatment resulted in a dual influence on the valorization of mustard seed meal, acting as a green solvent for oil recovery and increasing