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The lake, escarpment and mainstem group systems had narrow diel and seasonal CO2 concentration variability, while wetlands and vegetated impoundments had the widest ranges. Our high resolution spatio-temporal sampling was essential to identifying CO2 outgassing hotspots in these geomorphically diverse catchments. Overall, 95% of excess dissolved CO2 traversing the upper Blue Mountains Plateau was outgassed to the atmosphere.It is believed that the generation of odorous materials in manure-slurry pits during the storage can be reduc