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New high-performance photocatalytic materials are required to effectively treat water pollution. The effect of annealing temperature on the photocatalytic activities of tin dioxide (SnO₂) nanoparticles is investigated in this work. SnO₂ nanoparticles are prepared via a hydrothermal method and annealing at various temperatures ranging from as-prepared to 900 °C. The size of SnO₂ nanoparticles increases from 4 nm to 10 nm with an increase in annealing temperature. The photocatalytic properties of these nanoparticles are evaluated through