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The rapid progression of piezoelectric technology and the upgradation of electronic devices have resulted in a global increase in Pb-based piezoelectric ceramic materials. In this study, the feasibility of incorporating Pb into a PbZr(PO4)2 double orthophosphate structure was evaluated by investigating the interaction mechanism of the perovskite with phosphate. The unique combination of X-ray absorption spectroscopy, selected area electronic diffraction, and Pawley refinement revealed that Pb was incorporated into a hexagonal structure
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