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Fabrication of homojunctions is a cost-effective efficient way to enhance the photocatalytic performance of polymeric carbon nitride (CN), but the generation of defects upon synthesizing CN homojunctions and their roles in the homojunction fabrication were hardly reported. Herein, nitrogen-deficient CN homojunctions were simply synthesized by calcining dicyandiamide-loaded CN (prepared from urea and denoted as UCN) with dicyandiamide polymerizing into CN (denoted as DCN) and simultaneous formation of nitrogen vacancies in the surface of
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