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The present work describes the development of a fully automated method based on online solid phase extraction (SPE)-liquid chromatography-tandem mass spectrometry (LC-MS/MS) for the simultaneous analysis of multiple classes of pesticides or metabolites in drinking water (DW), surface water (SW), and wastewater effluents (WWEs). The target list covers 111 pesticides or metabolites of various properties and families. LC-MS/MS and online SPE parameters were optimized with regard to the sorbent type, mobile phase composition, wash volume, a
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