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This work was designed to prepare a novel NiS/KNbO3 p-n heterojunction composite for efficient photocatalytic nitrogen fixation under simulated sunlight. The NiS/KNbO3 photocatalyst was prepared through a two-step hydrothermal method. X-ray diffraction, Raman spectroscopy, X-ray photoelectron spectroscopy, scanning electron microscopy, and transmission electron microscopy analyses proved that NiS nanoparticles were closely decorated on the surface of KNbO3 nanorods, to facilitate the migration of electrons between the two semiconductors.
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