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© 2020 The Authors. The Kaohsiung Journal of Medical Sciences published by John Wiley Sons Australia on behalf of Kaohsiung Medical University.The larvae of two harmful insect species Tenebrio molitor and Leptinotarsa decemlineata were analyzed. The insects were sprayed with insecticides containing the active substances cyfluthrin and deltamethrin ( T. molitor ), and thiamethoxam and acetamiprid ( L. decemlineata ). The sprayed insect larvae were left for 24, 48 and 72 hours. Samples were then prepared using SPME fiber to identify
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