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The radon (222Rn) and thoron (220Rn) fluxes from the soil and building materials are the major contributors to their indoor levels. Hence, the measurement of radon and thoron exhalation rates from the source matrix becomes the foremost step in controlling the indoor radon and thoron exposure. It is a challenge to measure the exhalation rates without disturbing the natural conditions. The back-diffusion phenomenon modifies the exhalation rate. The work presented here is to measure the back-diffusion coefficient and takes it into consider