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The novel C/Fe-FeVO₄ composite photocatalyst were synthesized by using a two-step hydrothermal synthesis method. Through a detailed exploration on the chemical and phisical properties by some spectroscopic and analytical techniques, the as-prepared C/Fe-FeVO₄ exhibted a nanosheet and meso porosity structure. Accordingly, we further utilized this C/Fe-FeVO₄ composite as a photocatalist for degradating the notorious ciprofloxacin (CIP) under simulated solar light (SSL) irradiation. Due to its outstanding catalytic properties, the C/Fe-Fe