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Two new compounds, sodium copper nickel diorthophosphate, Na2CuNi(PO4)2 (I), and dimanganese copper diorthophosphate, Mn2Cu(PO4)2 (II), were synthesized hydrothermally, yielding single crystals, and were studied by X-ray diffraction. In the crystal structures, various transition metals of d-elements occupy symmetrically independent crystallographic positions with different coordination geometries. In the crystal structure of Na2NiCu(PO4)2, NiO6 and CuO6 octahedra share edges to form chains that PO4 groups link into a framework with cavi
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