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A rapid, cost-effective and accurate detection of heavy metal ions is crucial for human health monitoring and environmental protection. Surface-enhanced Raman spectroscopy (SERS) has become a reliable method due to its outstanding performance for the identification of contaminants. In this paper, silver phosphate microcubes (Ag3PO4) were fabricated using two different precipitation methods for ultrasensitive SERS detection of heavy metal ions. The use of an organic linker (BPy) with Ag3PO4 enabled the immobilization of Hg2+ and Pb2+ ions. The
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