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Hydrothermal liquefaction of woody biomass with catalysts was commonly applied in bio-energy research, but the effects of catalyst and solvent on yield and properties of bio-energy are not clear. In this work, the influences of catalyst and solvent on bio-energy production were studied, during which four solvents and three catalysts were used, and the liquefaction parameters were optimized by experimental and Machine learning (ML) method. Results show that the maximum yields of bio-oil and biochar are 65.0% and 32.0%, respectively, and the caloricva