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Lead-free perovskites are attracting increasing interest as nontoxic materials for advanced optoelectronic applications. Here, we report on a family of silver/bismuth bromide double perovskites with lower dimensionality obtained by incorporating phenethylammonium (PEA) as an organic spacer, leading to the realization of two-dimensional double perovskites in the form of (PEA)4AgBiBr8 (n = 1) and the first reported (PEA)2CsAgBiBr7 (n = 2). In contrast to the situation prevailing in lead halide perovskites, we find a rather weak influence o
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