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The relative standard deviation was less than 10 % for antibiotics in the foodstuff and water samples. The validated Cryo-SIPN-µSPE in conjunction with HPLC-UV, proved to be versatile, efficient and robust while its capability toward the trace determination of drugs residues in real-life samples is demonstrated in this work.A self-separating, analyte-compatible, and efficient clean-up method for QuEChERS extracts was designed and developed based on dispersive solid-phase extraction using a branched polyethylenimine and nanoscale CaSO4 f
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