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Three different composites were produced, based on zinc oxide and biochar (ZnO/biochar), varying the type of biomass (Salvinia molesta SM; exhausted husk of black wattle EH; and sugarcane bagasse S, with pyrolysis under mild conditions at 350 and 450 °C. Evaluation was made of the capacities of the composites for photocatalytic degradation of sulfamethoxazole antibiotic (SMX) and methyl orange dye (MO). The properties of the prepared composites were influenced by the biomass source, with larger crystallite size (S, lower band gap ener