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The phase stability of electrolyte matrix was improved by metal dopant materials which are Ni and Mn. The Ni-, Mn-doped LiAlO₂ and dopant-free LiAlO₂ were prepared by the mechanochemical process (MCP). The effects of dopant material, molar ratio and type of precursor were investigated after heat treatment at 700 and 800 °C. As a results, the Mn-doped LiAlO₂ prevents phase transition even at higher operating temperature. Also, the stability was increased when Mn4+ ion was adapted as a precursor source than Mn3+ ion and the minimum Mn con
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