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Ordered mesoporous MgO was synthesized via template method by using magnesium nitrate as a precursor and amphiphilic triblock copolymer Pluronic F127 as a template. The products were characterized by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM), and the Brunauer-Emmett-Teller (BET) method was used to calculate the specific surface areas. The effects of aging time, relative humidity, and magnesium nitrate content on the morphology and textural properties of the products were studied. When the aging time was 36