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tion for labor analgesia in the United States.The typical preparation route of carbon-supported metallic catalyst is complex and uneconomical. Herein, we reported a thiol-assisted one-pot method by using 3-mercaptopropionic acid (MPA) to synthesize carbon-supported metal nanoparticles catalysts for efficient electrocatalytic reduction of carbon dioxide (CO2 RR). We found that the synthesized Au-MPA/C catalyst achieves a maximum CO faradaic efficiency (FE) of 96.2% with its partial current density of -11.4 mA/cm2 , which is much higher t