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Stabilization of these complexes ended up being achieved by with the weakly coordinating anions [Al(ORF )4 ]- or [F2 ]- (RF = C(CF3 )3 ). The limitations of two synthesis routes starting from neutral Nb(arene)2 (arene = C6 H3 Me3 , C6 H5 myself) or [NEt4 ][M(CO)6 ] (M = Nb, Ta) were examined. All substances were analyzed by single crystal X-ray determination, vibrational and NMR spectroscopy. DFT computations had been executed to aid the experi
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