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Since moisture may frequently be present in many solvents, it is important to know the reactivity of a catalyst against water for catalytic reactions. In order to explore the stability and understand the transformation process of diphosphino-boryl-based PBP pincer platform, [PdClB(NCH2 Pt Bu2 )2 -o-C6 H4 ] (1) was treated with PdCl2 , HB(NCH2 PPh2 )2 -o-C6 H4 was reacted with [PdCl2 (cod)] (cod=cyclo-octa-1,5-diene) and [Pd2 (dba)3 ] (dba=dibenzylideneacetone), respectively, in the presence of water. Some novel palladium POP complexes, [P
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