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050 µg/mL for methamidophos, recovery between 90% and 102%, and stability at room temperature and at the autosampler between 80% and 120%. The analytical methodology was applied to 34 forensic cases. Carbofuran was found in a concentration ranging from 0.020 µg/mL to more than 5.0 µg/mL, aldicarb was found from 0.10 to 2.5 µg/mL, and methamidophos was found at a concentration greater than 5.0 µg/mL. In 62% of the cases the pesticides under study were used to commit suicide. Necropsy findings of pesticide poisoning are non-specific. Theref