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In parallel, spectra were also used to build an end-point detection model based on principal component analysis (PCA) for multivariate statistical process control (MSPC). The novel MEMS-FPI sensor combined with robust chemometric analysis proved to be a suitable and affordable alternative for online process monitoring, contributing to sustainability in the process industry.Miniaturization is one of the main requirements in the design of portable devices that allow in-field analysis. This is especially interesting in environmental monitor