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The reduction of [(dpp-bian)BBr] (1, dpp-bian = 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene) with dilithium naphthalenide in Et2O gives [(dpp-bian)BBrLi2(Et2O)2]2 (3). The treatment of [(dpp-bian)BONa] (5) and [(dpp-bian)Ge] (7) with sodium is accompanied by protonation of the acenaphthylene fragment and affords [(H-dpp-bian)BONa(dme)2Na(dme)3] (6) and [(H-dpp-bian)Ge][Na(dme)3] (8), respectively. Compounds 3, 6 and 8 have been characterized by 1H NMR and IR spectroscopy. The molecular structures of 3, [(dpp-bian)BOK] (4) and 8 hav
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