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The catalyst shows enhanced activity, greater stability, and higher selectivity with remarkable recyclability up to 92% for five consecutive cycles. The catalytic performance of the synthesized Pd NCs was also studied in the reduction of the organic contaminant p-NP, which showed an excellent performance screening of 99% conversion in 6 min.Electrocatalytic water splitting (EWS) is a key technology for generating clean and sustainable hydrogen, which can store abundant energy but is impeded by the insufficient efficiency of the anode and