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Furthermore, the feasibility of the proposed two-stage method in mixed dye pollutants removal (anionic and cationic) testified, which showed excellent performance even in doubling the dye pollutant concentration. This work brings a deeper insight into understanding the morphology and concentration of 2-D MoS2 in MoS2/TiO2 nanocomposite in tackling mixed dye pollutants and the possibilities of applying in textile dyeing industries wastewater treatment plants.Hexabromocyclododecane (HBCD) is one of the priority persistent organic pollutants (POPs), yet a cost