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Interestingly, when a dispersion with a water content of 50 vol % is diluted with a THF/H2O mixture with the same water content, the shapes of the JPs are significantly modified and vitrified after removal of THF through evaporation. By increasing the dilution multiples adopted to dilute the intermediate dispersions, JPs with more asymmetric shapes are obtained due to the enhanced asynchronous aggregation. Ternary phase diagrams calculated according to the Flory-Huggins theory provide a semi-quantitative description and rationalization of