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However, when the extracted Li+ further achieves a certain amount, after the high temperature heat-treatment the Mn-rich Li2MnO3 phase (C2/m) could be separated from Ni-rich phases (including R3m, Fd3m, and Fm3m), thus resulting in a sharp deterioration of initial capacity and voltage. These findings suggest that reheating the delithiated Li-rich material to high temperature may be a simple and effective way to improve the predelithiation modification method, but first the amount of extracted Li+ should be carefully optimized during the
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