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The system when it comes to photocurrent generation of nPCN-224 was systematically investigated, showing that the dissolved O2 in aqueous solution took part in the cost separation and transportation through the photoelectric conversion by generating O2˙-, which led to a 6-fold enhanced photocurrent using ascorbic acid as the O2 ˙- scavenger. Additionally, the built-in architectural porosity of nPCN-224 demonstrated advantage for reactant accessibility. Due to the exceptional properties of nPCN-224, together with
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