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In this study, we investigated the oxidation of acetaldehyde over Co/carbon black catalysts. All experiments were conducted in the temperature range of 200-440 °C, at an acetaldehyde concentration of 0.94 mol% in air, and using Co loading amounts in the range of 2-60 wt%. The nanosized carbon black and Co/carbon black catalysts were characterized using thermogravimetric analysis (TGA) and X-ray diffraction (XRD) analysis. The TGA data revealed that the nanosized carbon black was stable at high temperatures (600 °C), and the XRD res