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FT-IR spectra of poly(AN-co-EGDMA-co-VBC) show that the consumption rings at ~1290 cm-1 which can be assigned to the C-Cl oscillations are practically disappeared in hypercrosslinked (HXL) poly(AN-co-EGDMA-co-VBC) polymers, guaranteeing that the hypercrosslinking effect is prosperous . SEM pictures show that the morphologies associated with the polymers are retained through the hypercrosslinking reactions. Brunauer-Emmett-Teller (BET) evaluation shows that hypercrosslinked polymers had a particular su