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Alloys are active in CO2 electroreduction due to their unique electronic and geometric structures. Nevertheless, CO2 reduction selectivity is still low due to the low concentration of CO2 near the catalyst surface and the high energy barrier for CO2 activation. This paper describes an AuCu nanochain aerogel (NC-AuCu) with abundant grain boundaries (GBs) that promote the accumulation and activation of CO2 for further electrochemical reduction, employing in situ attenuated total reflection surface-enhanced infrared absorption spectroscopy
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