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The combined analysis of spectroscopic data upon deaggregation with ditopic Lewis bases unambiguously demonstrated the formation of stable 1 1 adducts, with higher binding constants in comparison to those related to monotopic species. Therefore, the present Lewis acidic, dinuclear complexes behave as molecular tweezers of ditopic guests having a strong Lewis basicity.Due to the poor heat-resistance and intrinsic weakness of the bridging moieties in aerogel matrixes, it remains greatly challenging to fabricate highly thermostable and t
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