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The influence of the incorporation of nanoparticles of titanium oxide (TiO2) at a concentration between 1000 and 50,000 ppm on the physicochemical and mechanical properties of a polymer matrix formed from a binary mixture of chitosan (CS) and polyvinyl alcohol (PVA) at a ratio of 8020 and the possibility of its use as a solid polymeric electrolyte were evaluated. With the mixture of the precursors, a membrane was formed with the solvent evaporation technique (casting). It was found that the incorporation of the nanoparticles affected the