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Recent water treatment plants require multi-process techniques to remove contaminants from aqua media. In this study, we investigate the novel, in situ coated sodium dodecylsulphate (SDS), on kegging Al30 nanocluster as a single water treatment alternative for the removal of phenolic contaminants and suspension. FTIR, TEM-EDX and Zeta potential analysis characterized the nanocluster decoration. The resulting property was examined by emission (λ-max) of the molecular probe, the online aggregate image of fluorescence microscopy, and mixing