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We report a heterogeneous postassembly modification (PAM) to synthesize a zirconium metal-organic cage decorated with acrylate functional groups, ZrT-1-AA, which cannot be synthesized by direct coordination-driven self-assembly owing to the reactivity and instability of the ligand. The PAM process is carried out in a single-crystal-to-single-crystal transformation under mild reaction conditions with high efficiency, which is confirmed by ESI-TOF-MS and 1H NMR. In addition, ZrT-1-AA is crosslinked into shaped materials to demonstrate it
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