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Alternating amphiphilic copolymers are macromolecular systems with a polarity duality in their structure, since they are generally formed by alternating segments corresponding to a potential electrolyte group and an alkyl (aliphatic or aromatic) group. These systems, depending on the ionization degree, as well as the time, may form different types of intra and interpolymeric aggregates in aqueous media. Therefore, this study, which in fact is the continuation of a previously reported work, is focused on establishing how the ionization d