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7% less than that prepared at 50% amplitude of ultrasonic irradiation. The particles of C60/Ga2O3 prepared by different modes of amplitude formed large (2-12 μm) aggregates in their solid phase.Whereas, in the aqueous medium, they were found to disperse in their nano sizes. The minimum particle size of the as-synthesized C60/Ga2O3 in an aqueous medium prepared by the proposed method of switching ultrasonic amplitude reached to approximately 467 nm. Comparatively, the minimum particle sizes were approximately 658 nm and 144 nm, using 25