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Controlling the shape and size of nanostructured materials has been a topic of interest in the field of material science for decades. In this work, the ferroelectric material SrxBa1-xNb2O6 (x = 0.32-0.82, SBN) was prepared by hydrothermal synthesis, and the morphology is controllably changed from cube-shaped to hollow-ended structures based on a fundamental understanding of the precursor chemistry. Synchrotron X-ray total scattering and PDF analysis was used to reveal the structure of the Nb-acid precursor, showing Lindqvist-like motifs.
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