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Interferences were investigated, and the addition of aldehydes produced a clear concentration-dependent decrease of the cyanide signal. Besides, the method offers an economical use of limited sample material by the simultaneous determination of cyanide, ethanol, and congener alcohols.Three D-A compounds were designed and synthesized based on a benzothiadiazole acceptor. Azepane (AP), iminodubenzyl (ID and iminostilbene (IS were used, respectively, as donors and installed on the 5-position of BTD to afford 1, 2 and 3, respectively. Th