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In this work, a multifunctional molybdate-phosphorus hierarchical hollow nanosphere (Mo-P-HH) catalyst had been successfully produced by a simple method followed by phosphorization. When compared to a commercial Pd/C catalyst, the multifunctional Mo-P-HH catalyst was far better in making water-soluble humic acid with small molecular practical teams from lignite via solid-phase activation. Moreover, Fourier change ion cyclotron resonance mass spectrome
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