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In the present work, an analytical method has been developed for the determination of the amount of man-made beryllium metal and/or beryllium compounds in soil in addition to the amount of native beryllium that is present. The method is based on the premise that if high-fired beryllium oxide can be extracted efficiently, then beryllium metal and acid-soluble beryllium salts would also be extracted efficiently. The proposed method involves the addition of 9 mL of an aqueous solution of 5% (wt/vol) ammonium bifluoride (ABF) to a 10-mL tu