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The fastest phenol degradation ended up being obtained with M (0.1%)/TiO2-P25, the reactivity order being Cu V Cr TiO2-P25 under 366 nm irradiation, while TiO2-P25 Cu V Cr, when using 254 nm radiation. TOC removal under 366 nm irradiation for 300 min showed very nearly quantitative mineralization for all tested materials, while 254 nm irradiation for 60 min resulted in maximum TOC removal (ca. 30%). Photoproducts and intermediate phot
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