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In this study, we have successfully synthesized honeycomb-like self-assembled structure of TiO2 modified ZnO/SnO2 nanostructure via co-precipitation method with exceptional high degradation activities for 2,4-dichlorophenol (2,4-DCP) and bisphenol A (BPA) pollutants. The as-prepared samples were calcined in tube furnace at high elevated temperature (700, 800 and 900 °C) for 1 h. Among the TiO2 modified samples, ZST10-700 showed higher charge separation as demonstrated from surface photovoltage spectroscopy, photoluminance and electrochemi